@Filename: C:\vsm-lv\Tarun\APL Fabrication paper and Batch 22 (ultrasound expts)\Thinfilmeaha\Thinfilmeaha-Hys-a000-00.VHD @Measurement Controlfilename: c:\vsm-lv\Reinoud\Recipes\Hys-a000-122.VHC @Calibration filename: c:\vsm-lv\Reinoud\settings\default.cal @Parameter Filec:\vsm-lv\Reinoud\settings\default.cal @Operator: Reinoud @Samplename: Thin film ea ha @Date: Tuesday, March 31, 2015 (2015-03-31) @Time: 13:56:39 @Test ID: SP4146 @Apparatus: EV X; SN: XXXXXXXX; Customer: XXXXXXXXX; first started on: Tuesday, January 25, 2011 VSM Model = EV X, Signal Processor = 2 SRS SR 830, Gaussmeter = 32 KP DRC, Gauss Probe = 1 x, VSM = TRUE, Torque = FALSE Rotation Card = TRUE, Rotation Display = FALSE, Rotate Option = Mdrive Temperature Control = TRUE, Temperature control Type = SI 9700, Thermocouple Type = J-type, Liquid Helium = FALSE, Boil Off Nitrogen = FALSE, Leave Temp On = FALSE Vector Coils = TRUE, Z Coils = FALSE, Stationary Coils = FALSE, Sensor Angle = 0 deg, Signal Connection = A-B @System Status = Online @Sample Orientation and Shape: line parallel with field @@Sample Dimensions Shape = Circular; Length = 6.60 [mm] Width = 6.60 [mm] Thickness = 1.000E+3 [nm] Diameter = 8.00 [mm] Volume : 5.027E-11 [m^3] Area = 5.027E+1 [mm^2] Mass = 1.000E+0 [g] Nd = 0.00 Sample Angle Offset = 0.000 Ms (for Hys loss calculation) = 1.000 [memu] @@End Sample Dimensions @Measurement type: Hysteresis Loop @Product of: MicroSense EasyVSM Software version 9.13U (January 27, 2011) @@Comments: @@END Comments @@Parameters @@Measurement Preparation Actions Action 0: Set Field Angle to 0.0000 [deg] and wait 0.0000 s ; Set Mode = Set and wait till there Action 1: Set Applied Field to -14999.0000 [Oe] and wait 0.0000 s ; Set Mode = Set and wait till there Action 2: Set Auto Range Signal to 10.0000 [ ] and wait 0.0000 s ; Set Mode = Set and wait till there @@END Measurement Preparation Actions @@Measurement Parameters @Repeat all sections = Symmetric @Number of sections= 3 @Section 0: Hysteresis; New Plot @Preparation Actions: Action 0: Set Gauss Range to 0.0000 [ ] and wait 0.0000 s ; Set Mode = Set and wait till there @Repeated Actions: Action 0: Set Applied Field to 0.0000 [Oe] and wait 0.0000 s ; Set Mode = Set and wait till there; Measure @Main Parameter = 0 : Applied Field [Oe]. @Main Parameter Setup: From: -15000.0000 [Oe] To: -4000.0000 [Oe] Min Stepsize/Sweeprate = 300.0000 [Oe] Max Stepsize/Sweeprate = 300.0000 [Oe] Signal change min step = 10.00 [%] Signal change max step = 0.00 [%] ; Wait time = 0.00 [sec] Up & Down = No @Measured Signal(s) = X & Y @Section 0 END @Section 1: Hysteresis @Main Parameter Setup: From: -4000.0000 [Oe] To: 4000.0000 [Oe] Min Stepsize/Sweeprate = 30.0000 [Oe] Max Stepsize/Sweeprate = 30.0000 [Oe] Signal change min step = 10.00 [%] Signal change max step = 0.00 [%] ; Wait time = 0.00 [sec] Up & Down = No @Section 1 END @Section 2: Hysteresis @Main Parameter Setup: From: 4000.0000 [Oe] To: 15000.0000 [Oe] Min Stepsize/Sweeprate = 300.0000 [Oe] Max Stepsize/Sweeprate = 300.0000 [Oe] Signal change min step = 10.00 [%] Signal change max step = 0.00 [%] ; Wait time = 0.00 [sec] Up & Down = No @Section 2 END @@Plot Settings Number of plots: 2 Plot 0: Hysteresis = On; Section: 0; Signal: X; Label: Hys X; Point style: 1; Interpolation: On; Color: 15663143; Mirror: Off Plot 1: Hysteresis = On; Section: 0; Signal: Y; Label: Hys Y; Point style: 0; Interpolation: On; Color: 0; Mirror: Off @@ENDPlot Settings @@END Measurement Parameters @@Instrument Parameters Stationary Coils = FALSE Sensor Angle = 0 deg @Gauss Range: 30 kOe @Emu Range: 5 uV @Torque Range: 4000 dyne cm @Auto-range emu: No @Number of averages: 10 @Rot 0 deg cal: -21000 @Rot 360 deg cal: 21000 @Dec Pt. constant: 1000 @Emu dec cal: 100 @Emdac: 28000 @Emu/v: 85.020 @Y Coils Correction Factor: 0.982 @Sample Shape Correction Factor: 1.000 @Coil Angle Alpha: 45.000 @Coil Angle Beta: -45.000 [Data Manipulation] Field Linearity Correction = No Image Effect 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344.000000 9.990028E-1 1.392167E+0 0.000000 345.000000 9.997340E-1 1.387451E+0 0.000000 346.000000 1.000345E+0 1.382931E+0 0.000000 347.000000 1.000842E+0 1.378596E+0 0.000000 348.000000 1.001233E+0 1.374432E+0 0.000000 349.000000 1.001526E+0 1.370427E+0 0.000000 350.000000 1.001730E+0 1.366567E+0 0.000000 351.000000 1.001853E+0 1.362838E+0 0.000000 352.000000 1.001903E+0 1.359229E+0 0.000000 353.000000 1.001888E+0 1.355725E+0 0.000000 354.000000 1.001815E+0 1.352313E+0 0.000000 355.000000 1.001694E+0 1.348981E+0 0.000000 356.000000 1.001533E+0 1.345714E+0 0.000000 357.000000 1.001338E+0 1.342501E+0 0.000000 358.000000 1.001120E+0 1.339327E+0 0.000000 359.000000 1.000885E+0 1.336179E+0 0.000000 360.000000 1.000642E+0 1.333044E+0 0.000000 Remove Slope = No Remove Signal Offset = No Remove Field Offset = No Cubic Spline Interpolation = No # Points = 0 Noise Filter = No Filter Order = 0 Filter Type = Median Subtract Files = No [Demagnetizing Field Correction] Demagnetizing Field Correction = No; Nd = 0.000 (x 4 Pi); Sample Mounted Perpendicular to Field = No Date and time of last calibration = Monday, December 15, 2014 12:24:59 @@END Instrument Parameters @@END Parameters @@Columns @Column Separator: @Column Contents: @Number of sections: 3 @Section 0 Column 0: Time since start, Time [s] Column 1: Raw Temperature, Sample Temperature [degC] Column 2: Temperature, Sample Temperature [degC] Column 3: Temperature 2, Sample Temperature [degC] Column 4: Raw Applied Field, Applied Field [Oe] Column 5: Applied Field, Applied Field [Oe] Column 6: Field Angle, Field Angle [deg] Column 7: Raw Applied Field For Plot , Applied Field [Oe] Column 8: Applied Field For Plot , Applied Field [Oe] Column 9: Raw Signal Mx, Moment as measured [memu] Column 10: Raw Signal My, Moment as measured [memu] Column 11: Signal X direction, Moment [emu] Column 12: Signal Y direction, Moment [emu] @@END Columns @@End of Header. Time_since_start Raw_Temperature Temperature Temperature_2 Raw_Applied_Field Applied_Field Field_Angle Raw_Applied_Field_For_Plot_ Applied_Field_For_Plot_ Raw_Signal_Mx Raw_Signal_My Signal_X_direction Signal_Y_direction @Time at start of measurement: 13:56:39 @@Data New Section: Section 0: 7.118000E+0 1.671060E+1 1.671060E+1 1.803121E+1 -1.500300E+4 -1.500300E+4 0.000000E+0 -1.500200E+4 -1.500200E+4 -2.550770E-1 2.647038E-2 -1.630507E-3 2.300912E-4 1.995300E+1 1.669769E+1 1.669769E+1 1.798239E+1 -1.470300E+4 -1.470300E+4 0.000000E+0 -1.470300E+4 -1.470300E+4 -2.621617E-1 2.720677E-2 -1.611157E-3 2.276906E-4 3.281500E+1 1.670669E+1 1.670669E+1 1.797860E+1 -1.440200E+4 -1.440200E+4 0.000000E+0 -1.440300E+4 -1.440300E+4 -2.682191E-1 2.404744E-2 -1.590692E-3 2.201819E-4 4.576400E+1 1.670989E+1 1.670989E+1 1.799029E+1 -1.410200E+4 -1.410200E+4 0.000000E+0 -1.410300E+4 -1.410300E+4 -2.742151E-1 2.392866E-2 -1.570165E-3 2.166512E-4 5.816200E+1 1.671151E+1 1.671151E+1 1.808920E+1 -1.380200E+4 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-1.300200E+4 0.000000E+0 -1.300000E+4 -1.300000E+4 -2.961185E-1 2.045654E-2 -1.494553E-3 1.996987E-4 5.312501E+3 1.672970E+1 1.672970E+1 1.805941E+1 -1.330200E+4 -1.330200E+4 0.000000E+0 -1.329900E+4 -1.329900E+4 -2.894276E-1 2.333876E-2 -1.514297E-3 2.068337E-4 5.322083E+3 1.673229E+1 1.673229E+1 1.804110E+1 -1.360100E+4 -1.360100E+4 0.000000E+0 -1.359900E+4 -1.359900E+4 -2.849343E-1 2.425331E-2 -1.536326E-3 2.114055E-4 5.332151E+3 1.674130E+1 1.674130E+1 1.805389E+1 -1.390100E+4 -1.390100E+4 0.000000E+0 -1.390000E+4 -1.390000E+4 -2.747199E-1 2.478382E-2 -1.552723E-3 2.154861E-4 5.342251E+3 1.672509E+1 1.672509E+1 1.806451E+1 -1.420200E+4 -1.420200E+4 0.000000E+0 -1.420000E+4 -1.420000E+4 -2.709033E-1 2.535393E-2 -1.575429E-3 2.196073E-4 5.351903E+3 1.674221E+1 1.674221E+1 1.802941E+1 -1.450200E+4 -1.450200E+4 0.000000E+0 -1.449900E+4 -1.449900E+4 -2.657962E-1 2.580128E-2 -1.596756E-3 2.235566E-4 5.361525E+3 1.675649E+1 1.675649E+1 1.801840E+1 -1.480200E+4 -1.480200E+4 0.000000E+0 -1.479900E+4 -1.479900E+4 -2.590895E-1 2.305372E-2 -1.616572E-3 2.233371E-4 5.370622E+3 1.675970E+1 1.675970E+1 1.800350E+1 -1.500200E+4 -1.500200E+4 0.000000E+0 -1.499900E+4 -1.499900E+4 -2.564568E-1 2.552021E-2 -1.631622E-3 2.288143E-4 @@END Data. @Measurement parameters Upward Part Downward part Average Parameter 'definition' Hysteresis Loop Hysteresis Parameters Hc Oe 319.525 480.470 -80.472 Coercive Field: Field at which M//H changes sign Mr emu -33.649E-6 -50.054E-6 -8.203E-6 Remanent Magnetization: M at H=0 S 0.022 0.031 0.026 Squareness: Mr/Ms S* 0.455 0.347 0.401 1-(Mr/Hc)(1/slope at Hc) Ms emu 1.545E-3 -1.632E-3 1.588E-3 Saturation Magnetization: maximum M measured @END Measurement parameters