@Filename: C:\vsm-lv\Tarun\SP4133\particlesinh2o\particlesinh2o-Hys.VHD @Measurement Controlfilename: C:\vsm-lv\Reinoud\Recipes\Hys-2364.VHC @Calibration filename: c:\vsm-lv\Reinoud\settings\default.cal @Parameter Filec:\vsm-lv\Reinoud\settings\default.cal @Operator: Reinoud @Samplename: particles in h2o @Date: Thursday, February 19, 2015 (2015-02-19) @Time: 08:41:13 @Test ID: Batch 22 Ch @Apparatus: EV X; SN: XXXXXXXX; Customer: XXXXXXXXX; first started on: Tuesday, January 25, 2011 VSM Model = EV X, Signal Processor = 2 SRS SR 830, Gaussmeter = 32 KP DRC, Gauss Probe = 1 x, VSM = TRUE, Torque = FALSE Rotation Card = TRUE, Rotation Display = FALSE, Rotate Option = Mdrive Temperature Control = TRUE, Temperature control Type = SI 9700, Thermocouple Type = J-type, Liquid Helium = FALSE, Boil Off Nitrogen = FALSE, Leave Temp On = FALSE Vector Coils = TRUE, Z Coils = FALSE, Stationary Coils = FALSE, Sensor Angle = 0 deg, Signal Connection = A-B @System Status = Online @Sample Orientation and Shape: line parallel with field @@Sample Dimensions Shape = Circular; Length = 6.60 [mm] Width = 6.60 [mm] Thickness = 1.000E+3 [nm] Diameter = 8.00 [mm] Volume : 5.027E-11 [m^3] Area = 5.027E+1 [mm^2] Mass = 1.000E+0 [g] Nd = 0.00 Sample Angle Offset = 0.000 Ms (for Hys loss calculation) = 1.000 [memu] @@End Sample Dimensions @Measurement type: Hysteresis Loop @Product of: MicroSense EasyVSM Software version 9.13U (January 27, 2011) @@Comments: @@END Comments @@Parameters @@Measurement Preparation Actions Action 0: Set Field Angle to 0.0000 [deg] and wait 0.0000 s ; Set Mode = Set and wait till there Action 1: Set Applied Field to -14999.0000 [Oe] and wait 0.0000 s ; Set Mode = Set and wait till there Action 2: Set Auto Range Signal to 13.0000 [ ] and wait 0.0000 s ; Set Mode = Set and wait till there @@END Measurement Preparation Actions @@Measurement Parameters @Repeat all sections = Symmetric @Number of sections= 3 @Section 0: Hysteresis; New Plot @Preparation Actions: Action 0: Set Gauss Range to 0.0000 [ ] and wait 0.0000 s ; Set Mode = Set and wait till there @Repeated Actions: Action 0: Set Applied Field to 0.0000 [Oe] and wait 0.0000 s ; Set Mode = Set and wait till there; Measure @Main Parameter = 0 : Applied Field [Oe]. @Main Parameter Setup: From: -15000.0000 [Oe] To: -4000.0000 [Oe] Min Stepsize/Sweeprate = 300.0000 [Oe] Max Stepsize/Sweeprate = 300.0000 [Oe] Signal change min step = 0.00 [%] Signal change max step = 0.00 [%] ; Wait time = 0.00 [sec] Up & Down = No @Measured Signal(s) = X & Y @Section 0 END @Section 1: Hysteresis @Main Parameter Setup: From: -4000.0000 [Oe] To: 4000.0000 [Oe] Min Stepsize/Sweeprate = 30.0000 [Oe] Max Stepsize/Sweeprate = 30.0000 [Oe] Signal change min step = 0.00 [%] Signal change max step = 0.00 [%] ; Wait time = 0.00 [sec] Up & Down = No @Section 1 END @Section 2: Hysteresis @Main Parameter Setup: From: 4000.0000 [Oe] To: 15000.0000 [Oe] Min Stepsize/Sweeprate = 300.0000 [Oe] Max Stepsize/Sweeprate = 300.0000 [Oe] Signal change min step = 0.00 [%] Signal change max step = 0.00 [%] ; Wait time = 0.00 [sec] Up & Down = No @Section 2 END @@Plot Settings Number of plots: 2 Plot 0: Hysteresis = On; Section: 0; Signal: X; Label: Hys X; Point style: 1; Interpolation: On; Color: 15663143; Mirror: Off Plot 1: Hysteresis = On; Section: 0; Signal: Y; Label: Hys Y; Point style: 0; Interpolation: On; Color: 0; Mirror: Off @@ENDPlot Settings @@END Measurement Parameters @@Instrument Parameters Stationary Coils = FALSE Sensor Angle = 0 deg @Gauss Range: 30 kOe @Emu Range: 50 uV @Torque Range: 4000 dyne cm @Auto-range emu: No @Number of averages: 10 @Rot 0 deg cal: -21000 @Rot 360 deg cal: 21000 @Dec Pt. constant: 1000 @Emu dec cal: 100 @Emdac: 28000 @Emu/v: 85.020 @Y Coils Correction Factor: 0.982 @Sample Shape Correction Factor: 1.000 @Coil Angle Alpha: 45.000 @Coil Angle Beta: -45.000 [Data Manipulation] Field Linearity Correction = No Image Effect Correction = Yes Image Correction Array Length = 23 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8.842492E-1 1.731895E+0 0.000000 301.000000 8.872092E-1 1.714422E+0 0.000000 302.000000 8.902283E-1 1.699064E+0 0.000000 303.000000 8.933008E-1 1.685626E+0 0.000000 304.000000 8.964216E-1 1.673914E+0 0.000000 305.000000 8.995853E-1 1.663734E+0 0.000000 306.000000 9.027864E-1 1.654894E+0 0.000000 307.000000 9.060196E-1 1.647197E+0 0.000000 308.000000 9.092796E-1 1.640451E+0 0.000000 309.000000 9.125610E-1 1.634461E+0 0.000000 310.000000 9.158583E-1 1.629034E+0 0.000000 311.000000 9.191664E-1 1.623976E+0 0.000000 312.000000 9.224797E-1 1.619092E+0 0.000000 313.000000 9.257929E-1 1.614188E+0 0.000000 314.000000 9.291008E-1 1.609071E+0 0.000000 315.000000 9.323978E-1 1.603546E+0 0.000000 316.000000 9.356785E-1 1.597462E+0 0.000000 317.000000 9.389371E-1 1.590836E+0 0.000000 318.000000 9.421676E-1 1.583725E+0 0.000000 319.000000 9.453641E-1 1.576190E+0 0.000000 320.000000 9.485205E-1 1.568288E+0 0.000000 321.000000 9.516310E-1 1.560078E+0 0.000000 322.000000 9.546896E-1 1.551620E+0 0.000000 323.000000 9.576902E-1 1.542972E+0 0.000000 324.000000 9.606270E-1 1.534192E+0 0.000000 325.000000 9.634941E-1 1.525340E+0 0.000000 326.000000 9.662853E-1 1.516475E+0 0.000000 327.000000 9.689948E-1 1.507654E+0 0.000000 328.000000 9.716166E-1 1.498937E+0 0.000000 329.000000 9.741448E-1 1.490383E+0 0.000000 330.000000 9.765734E-1 1.482050E+0 0.000000 331.000000 9.788972E-1 1.473987E+0 0.000000 332.000000 9.811143E-1 1.466199E+0 0.000000 333.000000 9.832237E-1 1.458679E+0 0.000000 334.000000 9.852243E-1 1.451424E+0 0.000000 335.000000 9.871149E-1 1.444427E+0 0.000000 336.000000 9.888945E-1 1.437682E+0 0.000000 337.000000 9.905619E-1 1.431185E+0 0.000000 338.000000 9.921162E-1 1.424929E+0 0.000000 339.000000 9.935561E-1 1.418910E+0 0.000000 340.000000 9.948806E-1 1.413122E+0 0.000000 341.000000 9.960886E-1 1.407559E+0 0.000000 342.000000 9.971791E-1 1.402216E+0 0.000000 343.000000 9.981508E-1 1.397087E+0 0.000000 344.000000 9.990028E-1 1.392167E+0 0.000000 345.000000 9.997340E-1 1.387451E+0 0.000000 346.000000 1.000345E+0 1.382931E+0 0.000000 347.000000 1.000842E+0 1.378596E+0 0.000000 348.000000 1.001233E+0 1.374432E+0 0.000000 349.000000 1.001526E+0 1.370427E+0 0.000000 350.000000 1.001730E+0 1.366567E+0 0.000000 351.000000 1.001853E+0 1.362838E+0 0.000000 352.000000 1.001903E+0 1.359229E+0 0.000000 353.000000 1.001888E+0 1.355725E+0 0.000000 354.000000 1.001815E+0 1.352313E+0 0.000000 355.000000 1.001694E+0 1.348981E+0 0.000000 356.000000 1.001533E+0 1.345714E+0 0.000000 357.000000 1.001338E+0 1.342501E+0 0.000000 358.000000 1.001120E+0 1.339327E+0 0.000000 359.000000 1.000885E+0 1.336179E+0 0.000000 360.000000 1.000642E+0 1.333044E+0 0.000000 Remove Slope = No Remove Signal Offset = No Remove Field Offset = No Cubic Spline Interpolation = No # Points = 0 Noise Filter = No Filter Order = 0 Filter Type = Median Subtract Files = No [Demagnetizing Field Correction] Demagnetizing Field Correction = No; Nd = 0.000 (x 4 Pi); Sample Mounted Perpendicular to Field = No Date and time of last calibration = Monday, December 15, 2014 12:24:59 @@END Instrument Parameters @@END Parameters @@Columns @Column Separator: @Column Contents: @Number of sections: 3 @Section 0 Column 0: Time since start, Time [s] Column 1: Raw Temperature, Sample Temperature [degC] Column 2: Temperature, Sample Temperature [degC] Column 3: Temperature 2, Sample Temperature [degC] Column 4: Raw Applied Field, Applied Field [Oe] Column 5: Applied Field, Applied Field [Oe] Column 6: Field Angle, Field Angle [deg] Column 7: Raw Applied Field For Plot , Applied Field [Oe] Column 8: Applied Field For Plot , Applied Field [Oe] Column 9: Raw Signal Mx, Moment as measured [memu] Column 10: Raw Signal My, Moment as measured [memu] Column 11: Signal X direction, Moment [emu] Column 12: Signal Y direction, Moment [emu] @@END Columns @@End of Header. Time_since_start Raw_Temperature Temperature Temperature_2 Raw_Applied_Field Applied_Field Field_Angle Raw_Applied_Field_For_Plot_ Applied_Field_For_Plot_ Raw_Signal_Mx Raw_Signal_My Signal_X_direction Signal_Y_direction @Time at start of measurement: 08:41:13 @@Data New Section: Section 0: 6.016000E+0 1.596331E+1 1.596331E+1 1.756631E+1 -1.500200E+4 -1.500200E+4 0.000000E+0 -1.500200E+4 -1.500200E+4 2.552031E+0 7.813617E-2 1.176601E-3 2.976874E-4 1.895600E+1 1.595641E+1 1.595641E+1 1.760870E+1 -1.470200E+4 -1.470200E+4 0.000000E+0 -1.470200E+4 -1.470200E+4 2.497458E+0 7.476307E-2 1.148551E-3 2.898990E-4 3.158900E+1 1.595831E+1 1.595831E+1 1.756600E+1 -1.440200E+4 -1.440200E+4 0.000000E+0 -1.440200E+4 -1.440200E+4 2.444963E+0 7.248264E-2 1.122578E-3 2.835401E-4 4.501100E+1 1.596331E+1 1.596331E+1 1.755511E+1 -1.410200E+4 -1.410200E+4 0.000000E+0 -1.410200E+4 -1.410200E+4 2.394269E+0 7.007554E-2 1.098408E-3 2.770156E-4 5.788900E+1 1.595361E+1 1.595361E+1 1.755959E+1 -1.380100E+4 -1.380100E+4 0.000000E+0 -1.380200E+4 -1.380200E+4 2.346161E+0 7.089901E-2 1.076822E-3 2.747177E-4 7.002500E+1 1.595791E+1 1.595791E+1 1.758679E+1 -1.350200E+4 -1.350200E+4 0.000000E+0 -1.350200E+4 -1.350200E+4 2.294297E+0 7.045561E-2 1.051481E-3 2.707623E-4 8.245400E+1 1.595941E+1 1.595941E+1 1.763409E+1 -1.320200E+4 -1.320200E+4 0.000000E+0 -1.320300E+4 -1.320300E+4 2.240801E+0 6.695581E-2 1.024419E-3 2.628193E-4 9.485000E+1 1.595980E+1 1.595980E+1 1.759060E+1 -1.290200E+4 -1.290200E+4 0.000000E+0 -1.290300E+4 -1.290300E+4 2.187988E+0 6.613231E-2 9.981292E-4 2.583666E-4 1.069670E+2 1.596209E+1 1.596209E+1 1.761981E+1 -1.260200E+4 -1.260200E+4 0.000000E+0 -1.260300E+4 -1.260300E+4 2.132767E+0 6.359852E-2 9.694306E-4 2.516763E-4 1.188890E+2 1.596911E+1 1.596911E+1 1.760641E+1 -1.230200E+4 -1.230200E+4 0.000000E+0 -1.230200E+4 -1.230200E+4 2.078797E+0 6.393109E-2 9.420720E-4 2.487249E-4 1.299370E+2 1.596389E+1 1.596389E+1 1.762231E+1 -1.200200E+4 -1.200200E+4 0.000000E+0 -1.200200E+4 -1.200200E+4 2.025191E+0 6.106473E-2 9.149888E-4 2.415994E-4 1.418260E+2 1.596899E+1 1.596899E+1 1.766909E+1 -1.170200E+4 -1.170200E+4 0.000000E+0 -1.170200E+4 -1.170200E+4 1.973011E+0 5.872097E-2 8.893314E-4 2.351577E-4 1.523990E+2 1.596401E+1 1.596401E+1 1.763009E+1 -1.140200E+4 -1.140200E+4 0.000000E+0 -1.140200E+4 -1.140200E+4 1.917601E+0 5.864180E-2 8.604442E-4 2.316789E-4 1.643080E+2 1.596539E+1 1.596539E+1 1.756811E+1 -1.110200E+4 -1.110200E+4 0.000000E+0 -1.110200E+4 -1.110200E+4 1.867447E+0 5.590212E-2 8.368137E-4 2.247192E-4 1.748950E+2 1.596099E+1 1.596099E+1 1.751599E+1 -1.080200E+4 -1.080200E+4 0.000000E+0 -1.080200E+4 -1.080200E+4 1.810739E+0 5.575962E-2 8.066281E-4 2.211575E-4 1.859360E+2 1.596069E+1 1.596069E+1 1.749221E+1 -1.050200E+4 -1.050200E+4 0.000000E+0 -1.050200E+4 -1.050200E+4 1.760838E+0 5.381174E-2 7.832501E-4 2.152337E-4 1.959930E+2 1.597500E+1 1.597500E+1 1.749981E+1 -1.020100E+4 -1.020100E+4 0.000000E+0 -1.020200E+4 -1.020200E+4 1.704983E+0 5.389091E-2 7.539173E-4 2.119620E-4 2.064100E+2 1.598251E+1 1.598251E+1 1.751541E+1 -9.901000E+3 -9.901000E+3 0.000000E+0 -9.902000E+3 -9.902000E+3 1.650015E+0 5.086622E-2 7.254730E-4 2.046294E-4 2.158390E+2 1.599090E+1 1.599090E+1 1.750460E+1 -9.601000E+3 -9.601000E+3 0.000000E+0 -9.602000E+3 -9.602000E+3 1.599056E+0 5.092956E-2 7.010365E-4 2.013370E-4 2.266970E+2 1.598940E+1 1.598940E+1 1.750302E+1 -9.301000E+3 -9.301000E+3 0.000000E+0 -9.302000E+3 -9.302000E+3 1.543518E+0 4.807904E-2 6.720208E-4 1.942323E-4 2.365710E+2 1.600369E+1 1.600369E+1 1.749871E+1 -9.001000E+3 -9.001000E+3 0.000000E+0 -9.002000E+3 -9.002000E+3 1.491813E+0 4.735056E-2 6.468387E-4 1.899039E-4 2.473860E+2 1.600381E+1 1.600381E+1 1.746230E+1 -8.701000E+3 -8.701000E+3 0.000000E+0 -8.702000E+3 -8.702000E+3 1.438000E+0 4.442088E-2 6.195490E-4 1.826956E-4 2.572650E+2 1.600509E+1 1.600509E+1 1.750079E+1 -8.401000E+3 -8.401000E+3 0.000000E+0 -8.402000E+3 -8.402000E+3 1.381861E+0 4.571945E-2 5.899322E-4 1.810193E-4 2.675930E+2 1.601571E+1 1.601571E+1 1.750601E+1 -8.101000E+3 -8.101000E+3 0.000000E+0 -8.101000E+3 -8.101000E+3 1.324898E+0 4.305896E-2 5.595808E-4 1.741520E-4 2.770080E+2 1.601821E+1 1.601821E+1 1.753951E+1 -7.801000E+3 -7.801000E+3 0.000000E+0 -7.802000E+3 -7.802000E+3 1.273237E+0 4.100020E-2 5.343537E-4 1.680944E-4 2.868390E+2 1.602749E+1 1.602749E+1 1.751449E+1 -7.501000E+3 -7.501000E+3 0.000000E+0 -7.501000E+3 -7.501000E+3 1.223384E+0 4.093683E-2 5.111126E-4 1.646250E-4 2.967210E+2 1.603649E+1 1.603649E+1 1.748440E+1 -7.201000E+3 -7.201000E+3 0.000000E+0 -7.202000E+3 -7.202000E+3 1.167799E+0 4.003413E-2 4.819617E-4 1.600799E-4 3.078350E+2 1.603561E+1 1.603561E+1 1.750649E+1 -6.902000E+3 -6.902000E+3 0.000000E+0 -6.902000E+3 -6.902000E+3 1.115017E+0 3.860883E-2 4.557024E-4 1.548398E-4 3.177570E+2 1.604791E+1 1.604791E+1 1.751489E+1 -6.601000E+3 -6.601000E+3 0.000000E+0 -6.602000E+3 -6.602000E+3 1.062519E+0 3.550492E-2 4.297270E-4 1.474036E-4 3.271840E+2 1.604690E+1 1.604690E+1 1.750811E+1 -6.301000E+3 -6.301000E+3 0.000000E+0 -6.302000E+3 -6.302000E+3 1.007584E+0 3.350959E-2 4.013150E-4 1.414178E-4 3.363750E+2 1.606191E+1 1.606191E+1 1.757269E+1 -6.001000E+3 -6.001000E+3 0.000000E+0 -6.002000E+3 -6.002000E+3 9.564639E-1 3.322451E-2 3.767178E-4 1.376695E-4 3.458110E+2 1.605139E+1 1.605139E+1 1.757470E+1 -5.701000E+3 -5.701000E+3 0.000000E+0 -5.702000E+3 -5.702000E+3 9.007997E-1 3.075407E-2 3.475763E-4 1.310621E-4 3.551900E+2 1.606289E+1 1.606289E+1 1.754131E+1 -5.401000E+3 -5.401000E+3 0.000000E+0 -5.402000E+3 -5.402000E+3 8.475114E-1 2.912294E-2 3.208109E-4 1.255527E-4 3.646240E+2 1.606191E+1 1.606191E+1 1.751461E+1 -5.101000E+3 -5.101000E+3 0.000000E+0 -5.102000E+3 -5.102000E+3 7.938107E-1 2.779271E-2 2.936330E-4 1.204370E-4 3.739680E+2 1.605959E+1 1.605959E+1 1.752230E+1 -4.801000E+3 -4.801000E+3 0.000000E+0 -4.802000E+3 -4.802000E+3 7.414246E-1 2.589236E-2 2.677697E-4 1.145755E-4 3.833080E+2 1.607781E+1 1.607781E+1 1.753900E+1 -4.501000E+3 -4.501000E+3 0.000000E+0 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-1.500200E+4 2.552031E+0 7.813617E-2 1.176601E-3 2.976874E-4 1.895600E+1 1.595641E+1 1.595641E+1 1.760870E+1 -1.470200E+4 -1.470200E+4 0.000000E+0 -1.470200E+4 -1.470200E+4 2.497458E+0 7.476307E-2 1.148551E-3 2.898990E-4 3.158900E+1 1.595831E+1 1.595831E+1 1.756600E+1 -1.440200E+4 -1.440200E+4 0.000000E+0 -1.440200E+4 -1.440200E+4 2.444963E+0 7.248264E-2 1.122578E-3 2.835401E-4 4.501100E+1 1.596331E+1 1.596331E+1 1.755511E+1 -1.410200E+4 -1.410200E+4 0.000000E+0 -1.410200E+4 -1.410200E+4 2.394269E+0 7.007554E-2 1.098408E-3 2.770156E-4 5.788900E+1 1.595361E+1 1.595361E+1 1.755959E+1 -1.380100E+4 -1.380100E+4 0.000000E+0 -1.380200E+4 -1.380200E+4 2.346161E+0 7.089901E-2 1.076822E-3 2.747177E-4 7.002500E+1 1.595791E+1 1.595791E+1 1.758679E+1 -1.350200E+4 -1.350200E+4 0.000000E+0 -1.350200E+4 -1.350200E+4 2.294297E+0 7.045561E-2 1.051481E-3 2.707623E-4 8.245400E+1 1.595941E+1 1.595941E+1 1.763409E+1 -1.320200E+4 -1.320200E+4 0.000000E+0 -1.320300E+4 -1.320300E+4 2.240801E+0 6.695581E-2 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-1.270200E+4 0.000000E+0 -1.269900E+4 -1.269900E+4 2.144771E+0 6.356684E-2 9.729482E-4 2.527150E-4 5.269095E+3 1.638259E+1 1.638259E+1 1.768899E+1 -1.300200E+4 -1.300200E+4 0.000000E+0 -1.299900E+4 -1.299900E+4 2.197315E+0 6.258502E-2 9.989686E-4 2.548057E-4 5.278151E+3 1.639410E+1 1.639410E+1 1.766290E+1 -1.330100E+4 -1.330100E+4 0.000000E+0 -1.329900E+4 -1.329900E+4 2.251618E+0 6.488126E-2 1.026749E-3 2.611852E-4 5.287743E+3 1.639431E+1 1.639431E+1 1.770379E+1 -1.360100E+4 -1.360100E+4 0.000000E+0 -1.359900E+4 -1.359900E+4 2.303339E+0 6.747840E-2 1.051947E-3 2.679584E-4 5.297870E+3 1.640441E+1 1.640441E+1 1.772759E+1 -1.390100E+4 -1.390100E+4 0.000000E+0 -1.389900E+4 -1.389900E+4 2.357009E+0 6.635404E-2 1.079095E-3 2.698627E-4 5.307971E+3 1.639941E+1 1.639941E+1 1.768679E+1 -1.420100E+4 -1.420100E+4 0.000000E+0 -1.419900E+4 -1.419900E+4 2.406924E+0 6.936291E-2 1.102487E-3 2.771746E-4 5.317596E+3 1.640899E+1 1.640899E+1 1.767971E+1 -1.450200E+4 -1.450200E+4 0.000000E+0 -1.449900E+4 -1.449900E+4 2.462399E+0 7.093069E-2 1.131438E-3 2.826010E-4 5.327200E+3 1.641680E+1 1.641680E+1 1.768411E+1 -1.480100E+4 -1.480100E+4 0.000000E+0 -1.479900E+4 -1.479900E+4 2.513201E+0 7.099405E-2 1.155718E-3 2.860592E-4 5.336302E+3 1.641061E+1 1.641061E+1 1.767059E+1 -1.500100E+4 -1.500100E+4 0.000000E+0 -1.499900E+4 -1.499900E+4 2.547549E+0 7.221342E-2 1.172384E-3 2.899047E-4 @@END Data. @Measurement parameters Upward Part Downward part Average Parameter 'definition' Hysteresis Loop Hysteresis Parameters Hc Oe -15002.000 -14999.000 -1.500 Coercive Field: Field at which M//H changes sign Mr emu -42.238E-6 -41.342E-6 447.944E-9 Remanent Magnetization: M at H=0 S 0.036 0.033 0.034 Squareness: Mr/Ms S* 1.029 1.034 1.032 1-(Mr/Hc)(1/slope at Hc) Ms emu 1.177E-3 -1.253E-3 1.215E-3 Saturation Magnetization: maximum M measured @END Measurement parameters