This README.txt file was generated on 2022-10-10 by Jamie W. Gittins GENERAL INFORMATION 1. Title of Dataset: Research data supporting "Enhancing the energy storage performances of metal–organic frameworks by controlling microstructure". 2. Author Information A. Principal Investigator Contact Information Name: Dr Alexander C. Forse Institution: Yusuf Hamied Department of Chemistry, University of Cambridge Email: acf50@cam.ac.uk B. Associate or Co-investigator Contact Information Name: Jamie Gittins Institution: Yusuf Hamied Department of Chemistry, University of Cambridge Email: jwg37@cam.ac.uk 3. Date of data collection: 2020-11-13 to 2022-04-14 4. Geographic location of data collection: - University of Cambridge, Cambridgeshire, United Kingdom - Diamond Light Source, Didcot, Oxfordshire, United Kingdom 5. Information about funding sources that supported the collection of the data: See DOI: 10.1039/D2SC03389E for more information about funding that supported this work. SHARING/ACCESS INFORMATION 1. Licenses/restrictions placed on the data: CC BY License. 2. Links to publications that cite or use the data: DOI: 10.1039/D2SC03389E. 3. Was data derived from another source? NO 4. Recommended citation for this dataset: Gittins, J. W. et al. Research data supporting "Enhancing the energy storage performances of metal–organic frameworks by controlling microstructure". Cambridge Research Repository, Apollo, 2022, https://doi.org/10.17863/CAM.82440. DATA & FILE OVERVIEW 1. File List: This data set contains six primary files: - Conductivity Measurement Data (.xlsx, .txt - contains results from the measurements used to calculate conductivity values). - Electrochemistry Data (.txt - contains CV, GCD and EIS data from electrocehmcial cells assembled with a variety of different samples and either 1 M NEt4BF4 in ACN or EMIM-BF4 IL electrolytes, along with the metafiles for the cells). - Elemental Analysis Data (.pdf, .xlsx, .txt - contains elemental analysis data). - Gas Sorption Data (.txt - contains results from gas sorption measurements). - SEM Data (.tif - contains SEM images from a range of samples). - TEM Data (.tif, .txt - contains TEM images from samples of A-CuHHTP and B-CuHHTP, intesnity plot data for an image of B-CuHHTP, and results from simulations). - XRD Data (.txt - contains synchrotron XRD data). 2. Are there multiple versions of the dataset? NO METHODOLOGICAL INFORMATION 1. Description of methods used for collection/generation of data can be found at DOI: 10.1039/D2SC03389E. 2. Standard methods for processing the data were used. Please see DOI: 10.1039/d1ta04026 for more details. 3. Software needed to open the data: - .txt can be opened with any text editor. - .xlsx files can be opened with Microsoft Excel or any spreadsheet software. - .pdf files can be opened with any pdf viewer. - .tif files can be opened with an image viewer. 4. People involved with sample collection, processing, analysis and/or submission: See author list and acknowlegments of DOI: 10.1039/D2SC03389E. ADDITIONAL INFORMATION: If any additional information is required, please contact the corresponding author.