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Aberration-corrected and energy-filtered precession electron diffraction


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Type

Article

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Authors

Eggeman, AS 
Barnard, JS 
Midgley, PA 

Abstract

We report initial findings on improvements to precession electron diffraction (PED) achieved through aberration correction of the probe-forming lens and by energy-filtering. Using current-generation aberration correctors, we show that PED patterns can, in principle, be acquired with sub-nm spatial resolution. We present initial experimental results that illustrate aberration-corrected PED of nanostructured alloys. We show also that zero loss energy filtering minimizes the inelastic background in a PED pattern, important for weak reflections, and leads to an improvement in the refinement of a crystal structure using elastic-only intensities.

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Keywords

Electron crystallography, Aberration correction, Precession electron diffraction

Journal Title

Zeitschrift fur Kristallographie

Conference Name

Journal ISSN

0044-2968
2196-7105

Volume Title

Publisher

Walter de Gruyter GmbH
Sponsorship
Engineering and Physical Sciences Research Council (EP/H017712/1)
The authors would like to thank the EPSRC for financial support through grant number EP/H013378, and would like to thanks Rolls Royce plc, Dr Cathie Rae, Olivier Messe and Dr Michael Hardy for use of the nickel-based superalloy sample investigated in this study. PAM thanks the ERC for financial support through grant no. 291522 3DIMAGE.