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NMR reveals the surface functionalisation of Ti3C2 MXene.


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Authors

Hope, Michael A 
Forse, Alexander C 
Griffith, Kent J 
Lukatskaya, Maria R 
Ghidiu, Michael 

Abstract

(1)H and (19)F NMR experiments have identified and quantified the internal surface terminations of Ti3C2Tx MXene. -F and -OH terminations are shown to be intimately mixed and there are found to be significantly fewer -OH terminations than -F and -O, with the proportions highly dependent on the synthesis method.

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Keywords

0306 Physical Chemistry (incl. Structural), 1.1 Normal biological development and functioning

Journal Title

Phys Chem Chem Phys

Conference Name

Journal ISSN

1463-9076
1463-9084

Volume Title

18

Publisher

Royal Society of Chemistry (RSC)
Sponsorship
Engineering and Physical Sciences Research Council (EP/L019469/1)
Engineering and Physical Sciences Research Council (EP/K002252/1)
We are grateful for financial support by the Oppenheimer Foundation and EPSRC. Material synthesis and characterization at Drexel University was supported by the US National Science Foundation under grant number DMR-1310245.