Research data supporting "An Integrated Total Neutron Scattering - NMR Approach for the Study of Heterogeneous Catalysis"
Youngs, Tristan GA
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Leutzsch, M., Falkowska, M., Hughes, T., Sederman, A., Gladden, L., Mantle, M., Youngs, T. G., et al. (2022). Research data supporting "An Integrated Total Neutron Scattering - NMR Approach for the Study of Heterogeneous Catalysis" [Dataset]. https://doi.org/10.17863/CAM.24725
Nuclear magnetic resonance (NMR) and total neutron scattering techniques are established methods for the characterisation of liquid phases in confined pore spaces during chemical reactions. Herein, we describe the first combined total neutron scattering -NMR setup as a probe for the catalytic heterogeneous reduction of benzene-d6 with D2 in 3 wt.% Pt/MCM-41.
The raw 2H NMR data (NUTS format, http://ww.acornnmr.com) from the hydrogenation of benzene-d6 with D2 in 3wt.% Pt/MCM-41 acquired on an Oxford Instrument Pulsar 60 MHz NMR spectrometer was imported into Matlab (2016b) and processed therein. The name of the individual files was saved in the following format: Reactiontime(s)_Kinetic2H.fid
NeuNMR, Heterogeneous Catalysis, NMR, Total Neutron Scattering
Publication Reference: https://doi.org/10.1039/c8cc04740ehttps://www.repository.cam.ac.uk/handle/1810/280050
EPSRC: EP/N008995/1 Science and Technology Facilities Council for the allocated beam time at the ISIS Pulsed Neutron and Muon Source: RB1710475, DOI: 10.5286/ISIS.E.87813090
This record's DOI: https://doi.org/10.17863/CAM.24725
Attribution 4.0 International (CC BY 4.0)
Licence URL: https://creativecommons.org/licenses/by/4.0/