OriginLab dataset containing XRD, NMR and zeta potential data.

Figure 2 (XRD). X-ray diffraction (XRD) patterns of minerals produced by the reaction between calcium carbonate and orthophosphoric acid under a variety of synthesis time, pH conditions, and presence of citrate ions.

Figure 3 (XRD): XRD patterns of minerals produced by the hydrolysis of alpha-tricalcium phosphate under a variety of pH conditions (either maintained at or starting at 6.50) with a synthesis time of 24 hours (without citrate ions) or 28 hours (with citrate ions).

Figure 4 (NMR): Solid-state nuclear magnetic resonance spectra of powdered octacalcium phosphate (OCP) and OCP-citrate minerals (OCP-CIT) produced via the reaction between calcium carbonate and orthophosphoric acid or the hydrolysis of alpha-tricalcium phosphate, in 31P cross-polarisation, 31P high power decoupling and 13C{31P} Rotational Echo Double Resonance (REDOR) experiments.

Figure 5: The zeta potential and conductivity of mineralised collagen suspensions (OCP-CIT and collagen) before and after dialysis against DI water. The 13C{31P} REDOR spectra and XRD pattern of OCP-CIT after dialysis against DI water.

Figure 6: The zeta potential and conductivity of mineralised collagen suspensions (collagen mineralised with OCP-CIT (OCP-CIT/COLL) and collagen mineralised in the presence of hyaluronic acid (OCP-CIT/COLL/HyAc)) and collagen suspensions under a variety of hyaluronic acid concentrations and collagen suspension additions.

Figure 7: XRD patterns and solid-state NMR experiments (31P HPDEC and 31C{31} REDOR) of mineralised collagen films OCP-CIT/COLL and OCP-CIT/COLL/HyAc, and OCP-CIT mineral.